Hydrochloric Acid → HCID 178479039、化合物

HRID 849081

反応式

HRID 849081 の反応式
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH2:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[N:3]=1.[ClH:15]>[Pt]=O>[ClH:15].[CH:9]1([CH2:8][CH:4]2[NH:3][C:2](=[NH:1])[CH2:7][CH2:6][CH2:5]2)[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1

参加物

4

反応物 2

HCID 313Hydrochloric AcidHCID 939026-Benzylpyridin-2-amine

生成物 1

HCID 178479039HCID 178479039、化合物

試薬・触媒・溶媒 1

HCID 82844Platinum oxide (PtO)触媒

実験手順

The 2-amino-6-benzylpyridine was reduced as in Example 94, except platinum oxide was used as the catalyst. The product was obtained as an oil which was dissolved in 1 N HCl and lyophilized to give a white solid. The solid was recrystallized from EtOAc to give the desired title compound as white crystals. The analysis of the product was found to be consistent with the proposed structure.

後処理

  1. customThe product was obtained as an oil which
  2. customto give a white solid
  3. customThe solid was recrystallized from EtOAc

出典と根拠

ORDレコード
ord-ab961bebbe72482badb3276f57ec740a
出典データセット
uspto-grants-2000_01
特許番号
US06011028

関連ノート

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