2-Methylbenzimidazole → 1-(2-ethoxyethyl)-2-methyl-1H-benzimidazole

HRID 851842

反応式

HRID 851842 の反応式
[CH3:1][C:2]1[NH:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=1.[CH2:11]([O:13][CH2:14][CH2:15]Cl)[CH3:12]>>[CH2:11]([O:13][CH2:14][CH2:15][N:3]1[C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=[C:2]1[CH3:1])[CH3:12]

参加物

3

反応物 2

HCID 119842-MethylbenzimidazoleHCID 12341Ethane, 1-chloro-2-ethoxy-

生成物 1

HCID 19345641-(2-ethoxyethyl)-2-methyl-1H-benzimidazole収率 82%

実験手順

1-(2-Ethoxyethyl)-2-methyl-1H-benzimidazole was synthesized as in Synthesis Example 1 except that an equimolar amount of 2-methylbenzimidazole was used instead of benzimidazole, and an equimolar amount of 2-chloroethyl ethyl ether was used instead of 2-chloroethyl methyl ether. Yield 82%.

出典と根拠

ORDレコード
ord-d59419bd63c8448a8bb5968fd6619d97
出典データセット
uspto-grants-2007_08
特許番号
US07252925B2

関連ノート

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