HCID 21867058、化合物 → 6-[4-(3-Aminophenyl)butoxy]hexyl acetate
反応式
[C:1]([O:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][O:11][CH2:12][CH2:13][C:14]#[C:15][C:16]1[CH:21]=[CH:20][CH:19]=[C:18]([N+:22]([O-])=O)[CH:17]=1)(=[O:3])[CH3:2]>CCO.O=[Pt]=O>[C:1]([O:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][O:11][CH2:12][CH2:13][CH2:14][CH2:15][C:16]1[CH:21]=[CH:20][CH:19]=[C:18]([NH2:22])[CH:17]=1)(=[O:3])[CH3:2]参加物
4
実験手順
6-{[4-(3-Nitrophenyl)but-3-ynyl]oxy}hexyl acetate (2.973 g) was hydrogenated over PtO2 (300 mg) in EtOH over 1 h. The catalyst was removed by filtration and washed with EtOH. The combined filtrate and washings were concentrated under reduced pressure to give the title compound (2.844 g) LCMS RT=3.30 min.
後処理
- customThe catalyst was removed by filtration
- washwashed with EtOH
- concentrationThe combined filtrate and washings were concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-86418d09047148dd989cadad2369ca55
- 出典データセット
- uspto-grants-2006_12
- 特許番号
- US07144908B2
反応ノート
読み込み中…