化工社化工社 化学情報印刷レポート · 研究参考用
Methyl triflate → 1-Methyl-1H-indole-5-carboxylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl triflate | HCID 9526 | — |
| 反応物 | 1H-Indole-5-Carboxylic Acid | HCID 74280 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 1-Methyl-1H-indole-5-carboxylic acid | HCID 7015601 | — |
反応手順
0.1 g of indol-5-carboxylic acid was mixed with 2 equivalents of methyl trifluoromethane sulfonate in 1 ml DMF at room temperature. After 5 h the solvent was evaporated and 1H-NMR was recorded:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07148243B2 |
| 出典データセット | uspto-grants-2006_12 |
| ORD ID | ord-a0d26f19bf7a4baf960f448a6e4bd646 |
| 出典メモ | uspto-grants-2006_12 |