HRID858184

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID9526

Methyl trifluoromethanesulfonate

C2H3F3O3S

HCID74280

Indole-5-carboxylic acid

C9H7NO2

PRODUCTS

生成物

HCID7015601

1-methylindole-5-carboxylic Acid

C10H9NO2

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

0.1 g of indol-5-carboxylic acid was mixed with 2 equivalents of methyl trifluoromethane sulfonate in 1 ml DMF at room temperature. After 5 h the solvent was evaporated and 1H-NMR was recorded:

WORKUP

后处理

customAfter 5 h the solvent was evaporated