Water → HCID 22097227、化合物
反応式
[Cl:1][C:2]1[CH:7]=[C:6]([NH:8]C(=O)C)[C:5]([NH:12]C(=O)C)=[CH:4][C:3]=1[N:16]1[CH:20]=[CH:19][CH:18]=[CH:17]1.[OH-].[K+].O>C(O)CO>[Cl:1][C:2]1[CH:7]=[C:6]([NH2:8])[C:5]([NH2:12])=[CH:4][C:3]=1[N:16]1[CH:20]=[CH:19][CH:18]=[CH:17]1参加物
5
実験手順
A solution 1.4 g (4.8 mmol) of N-(2-chloro-4,5-diacetamidophenyl)pyrrole and 0.4 g (9.8 mmol) of potassium hydroxide in 25 ml of ethylene glycol was stirred at 60° C. for 30 minutes. The reaction mixture was then poured into water, extracted with ethyl acetate and worked up.
後処理
- extractionextracted with ethyl acetate
出典と根拠
- ORDレコード
- ord-a8ac6a40a8b8444cb5a77e6dadd6b87d
- 出典データセット
- uspto-grants-1998_02
- 特許番号
- US05714489
反応ノート
読み込み中…