HCID 4418042、化合物 → 2-N,2-N-diethylpyridine-2,5-diamine

HRID 861657ノート

反応式

HRID 861657 の反応式
[CH2:1]([N:3]([CH2:13][CH3:14])[C:4]1[CH:9]=[CH:8][C:7]([N+:10]([O-])=O)=[CH:6][N:5]=1)[CH3:2]>CO.[Pd]>[NH2:10][C:7]1[CH:8]=[CH:9][C:4]([N:3]([CH2:13][CH3:14])[CH2:1][CH3:2])=[N:5][CH:6]=1

参加物

4

反応物 1

HCID 4418042HCID 4418042、化合物

生成物 1

HCID 117884862-N,2-N-diethylpyridine-2,5-diamine収率 95%

試薬・触媒・溶媒 2

HCID 23938Palladium触媒HCID 887Methanol溶媒

実験手順

40 g of the 2-diethylamino-5-nitropyridine was subjected to catalytic reduction in one liter of methanol through the use of 2 g of 10% Pd-C. The catalyst was removed by filtration, and the filtrate was concentrated to give 32 g of 5-amino-2-diethylaminopyridine (yield: 95% oleaginous form).

後処理

  1. customThe catalyst was removed by filtration
  2. concentrationthe filtrate was concentrated

出典と根拠

ORDレコード
ord-98b4d69397f9412cba7d6391f3f49d1b
出典データセット
uspto-grants-1998_02
特許番号
US05714614

反応ノート

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