化工社化工社 化学情報印刷レポート · 研究参考用
Methyl iodide → Methyl 2-amino-6-chlorobenzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl iodide | HCID 6328 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 2-Amino-6-chlorobenzoic acid | HCID 75071 | — |
| 生成物 | Methyl 2-amino-6-chlorobenzoate | HCID 592849 | 78.4% |
反応手順
Using the procedure described above in Preparation 1, 5.0 g (0.029 mol) of 6-chloroanthranilic acid and 2.75 ml (0.044 mol) of iodomethane were reacted in the presence of 4.08 g (0.073 mol) of powdered potassium hydroxide to give 4.22 g (78%) of methyl 6-chloroanthranilate as an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05563163 |
| 出典データセット | uspto-grants-1996_10 |
| ORD ID | ord-8cd00d734c5444f1804c2288e1aabf23 |
| 出典メモ | uspto-grants-1996_10 |