4-Chlorophenyl Isocyanate → N-[[(4-chlorophenyl) amino]-carbonyl]-4-(4-morpholinyl) benzenesulfonamide

HRID 865316

反応式

HRID 865316 の反応式
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]=[C:9]=[O:10])=[CH:4][CH:3]=1.[N:11]1([C:17]2[CH:22]=[CH:21][C:20]([S:23]([NH2:26])(=[O:25])=[O:24])=[CH:19][CH:18]=2)[CH2:16][CH2:15][O:14][CH2:13][CH2:12]1>CC(C)=O>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]([NH:26][S:23]([C:20]2[CH:19]=[CH:18][C:17]([N:11]3[CH2:16][CH2:15][O:14][CH2:13][CH2:12]3)=[CH:22][CH:21]=2)(=[O:24])=[O:25])=[O:10])=[CH:4][CH:3]=1

参加物

4

反応物 2

HCID 76934-Chlorophenyl IsocyanateHCID 7354354-(Morpholin-4-yl)benzene-1-sulfonamide

生成物 1

HCID 15345719N-[[(4-chlorophenyl) amino]-carbonyl]-4-(4-morpholinyl) benzenesulfonamide

試薬・触媒・溶媒 1

HCID 180Acetone溶媒

実験手順

4-Chlorophenylisocyanate (2.61 g, 17 moles) was dissolved in 16 ml of acetone and was then added dropwise to the sulfonamide solution. The mixture was then stirred overnight at room temperature, resulting in the formation of a white solid.

後処理

  1. customresulting in the formation of a white solid

出典と根拠

ORDレコード
ord-fdccf3362d874d0bba3eb0d86506ba63
出典データセット
uspto-grants-1996_10
特許番号
US05565494

関連ノート

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