Ethyl 4-amino-1-piperidinecarboxylate → HCID 23374509、化合物

HRID 865647

反応式

HRID 865647 の反応式
[NH2:1][CH:2]1[CH2:7][CH2:6][N:5]([C:8]([O:10][CH2:11][CH3:12])=[O:9])[CH2:4][CH2:3]1.C(O[C:16]1[CH:21]=[CH:20][N:19]=[CH:18][C:17]=1[N+:22]([O-:24])=[O:23])C>CC#N>[N+:22]([C:17]1[CH:18]=[N:19][CH:20]=[CH:21][C:16]=1[NH:1][CH:2]1[CH2:3][CH2:4][N:5]([C:8]([O:10][CH2:11][CH3:12])=[O:9])[CH2:6][CH2:7]1)([O-:24])=[O:23]

参加物

4

反応物 2

HCID 100867Ethyl 4-amino-1-piperidinecarboxylateHCID 3563054-Ethoxy-3-nitropyridine

生成物 1

HCID 23374509HCID 23374509、化合物

試薬・触媒・溶媒 1

HCID 6342Acetonitrile溶媒

実験手順

A mixture of ethyl 4-amino-1-piperidinecarboxylate (3.53 g, 20.5 mmol) and 4-ethoxy-3-nitropyridine (3.65 g, 21/7 mmol) in CH3CN (25 mL) was heated at reflux for 40 hours. The reaction mixture was cooled to ambient temperature and concentrated in vacuo to give an orange syrup which was used without further purification.

後処理

  1. temperaturewas heated
  2. temperatureat reflux for 40 hours
  3. concentrationconcentrated in vacuo
  4. customto give an orange syrup which
  5. customwas used without further purification

出典と根拠

ORDレコード
ord-5b8ae9819dc8446a9b95b612a6523f32
出典データセット
uspto-grants-1996_10
特許番号
US05567711

関連ノート

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