Sodium Hydroxide → Atrinositol

HRID 867855

反応式

HRID 867855 の反応式
[CH:1]1([O:32][P:33]([O-:36])([O-:35])=[O:34])[CH:6]([O:7][P:8]([O-:11])([O-:10])=[O:9])[CH:5]([O:12][P:13]([O-:16])([O-:15])=[O:14])[CH:4]([O:17]P([O-])([O-])=O)[CH:3]([O:22]P([O-])([O-])=O)[CH:2]1[O:27]P([O-])([O-])=O.[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[OH-].[Na+]>C(O)C>[C@H:4]1([OH:17])[CH:3]([OH:22])[C@@H:2]([OH:27])[C@@H:1]([O:32][P:33]([OH:36])([OH:35])=[O:34])[CH:6]([O:7][P:8]([OH:10])([OH:11])=[O:9])[C@@H:5]1[O:12][P:13]([OH:15])([OH:16])=[O:14]

参加物

4

反応物 2

HCID 14798Sodium HydroxideHCID 66391Phytate Persodium

生成物 1

HCID 65762Atrinositol

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

100 ml of the fraction containing D-myo-inositol-1.2.6-triphosphate obtained in Example 15 was neutralized to a pH of about 7 with an aqueous solution of NaOH. After addition of 100 ml ethanol the volume of the solution was reduced by evaporation and the sodiumsalt was precipitated, centrifuged, recrystallized and dried in vacuum. The purified sodiumsalt of D-myo-inositol-1.2.6-triphosphate obtained was structurally confirmed by analysis with H-NMR.

後処理

  1. customwas reduced by evaporation
  2. customthe sodiumsalt was precipitated
  3. customrecrystallized
  4. customdried in vacuum

出典と根拠

ORDレコード
ord-9f33052edcde4fbab35e0f7266edce33
出典データセット
uspto-grants-1988_10
特許番号
US04777134

関連ノート

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