6-Methylbenzofuran → HCID 14257620、化合物

HRID 868613ノート

反応式

HRID 868613 の反応式
[CH3:1][C:2]1[CH:10]=[CH:9][C:5]2[CH:6]=[CH:7][O:8][C:4]=2[CH:3]=1.[H][H]>CO.[Pd]>[CH3:1][C:2]1[CH:10]=[CH:9][C:5]2[CH2:6][CH2:7][O:8][C:4]=2[CH:3]=1

参加物

5

反応物 2

HCID 869296-MethylbenzofuranHCID 178418361HCID 178418361、化合物

生成物 1

HCID 14257620HCID 14257620、化合物

試薬・触媒・溶媒 2

HCID 23938Palladium触媒HCID 887Methanol溶媒

実験手順

6-Methylbenzofuran (15 g) was dissolved in methanol (200 ml) containing 0.5 g of 10% palladium on carbon. This solution was shaken on a Paar hydrogenator under hydrogen at 40 psi. When hydrogen uptake was complete, the solution was filtered through Celite and the ethanol evaporated to yield 6-methyl-2,3-dihydrobenzofuran.

後処理

  1. filtrationthe solution was filtered through Celite
  2. customthe ethanol evaporated

出典と根拠

ORDレコード
ord-1957b114f40e408c93883833b0b7ccc0
出典データセット
uspto-grants-1988_10
特許番号
US04780480

反応ノート

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