Methyl iodide → 2-cyclopropyl-4-iodo-1-methyl-1H-imidazole

反応式

[CH:1]1([C:4]2[NH:5][C:6]([I:9])=[CH:7][N:8]=2)[CH2:3][CH2:2]1.I[CH3:11]>>[CH:1]1([C:4]2[N:8]([CH3:11])[CH:7]=[C:6]([I:9])[N:5]=2)[CH2:3][CH2:2]1

参加物

反応物 2

HCID 6328Methyl iodide

HCID 219853922-cyclopropyl-5-iodo-1H-imidazole

生成物 1

HCID 219853842-cyclopropyl-4-iodo-1-methyl-1H-imidazole

実験手順

The title compound, MS: m/e=249.1 (M+H+), was prepared in accordance with the general method of example 1 from 2-cyclopropyl-5-iodo-1H-imidazole (example C) and iodomethane.

出典と根拠

ORDレコード: ord-775a03628f4f4a1c86c6343eb6cf66fb
出典データセット: uspto-grants-2006_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07091222B2

反応ノート

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