Sodium Iodide → Cyclohexyloxycarbonyloxymethyl iodide
反応式
[C:1](=[O:12])([O:5][CH:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1)[O:2][CH2:3]Cl.[I-:13].[Na+]>CC(C)=O>[C:1](=[O:12])([O:5][CH:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1)[O:2][CH2:3][I:13]参加物
4
実験手順
A solution of 0.78 g of chloromethyl cyclohexyl carbonate and 1.0 g of sodium iodide in 15 ml of acetone is stirred at room temperature for 16 hours and then concentrated under reduced pressure. The residue is extracted with ether and the solvent is distilled off under reduced pressure to give the title compound as pale yellow oil.
後処理
- concentrationconcentrated under reduced pressure
- extractionThe residue is extracted with ether
- distillationthe solvent is distilled off under reduced pressure
出典と根拠
- ORDレコード
- ord-f6f0345371204717bf40763b7b156307
- 出典データセット
- uspto-grants-1992_06
- 特許番号
- US05120841
反応ノート
読み込み中…