Cyclohexene → 2-(2,5-Dimethylpyrrolidin-1-YL)-6-methoxypyrid-3-ylamine
反応式
[CH3:1][CH:2]1[CH2:6][CH2:5][CH:4]([CH3:7])[N:3]1[C:8]1[C:13]([N+:14]([O-])=O)=[CH:12][CH:11]=[C:10]([O:17][CH3:18])[N:9]=1.C1CCCCC=1>[Pd].C(O)C>[CH3:1][CH:2]1[CH2:6][CH2:5][CH:4]([CH3:7])[N:3]1[C:8]1[C:13]([NH2:14])=[CH:12][CH:11]=[C:10]([O:17][CH3:18])[N:9]=1参加物
5
実験手順
4.2 g (0.017 mol) of the product 2-(2,5-dimethylpyrrolidin-1-yl)-6-methoxy-3-nitropyridine synthesized according to the above procedure, 40 ml of ethanol, 10 ml of cyclohexene and 1.5 g of palladium-on-charcoal were placed in a fully equipped round-bottomed flask.
出典と根拠
- ORDレコード
- ord-0c01d60eec1f48449884218a77c64d8d
- 出典データセット
- uspto-grants-2005_07
- 特許番号
- US06916345B2
反応ノート
読み込み中…