Diisopropyl Ether → HCID 10291485、化合物
反応式
[OH:1][C:2]1[CH:3]=[CH:4][C:5]2[N:9]=[C:8]([C:10]([OH:12])=O)[NH:7][C:6]=2[CH:13]=1.C[CH:15]([CH:22]1[CH2:27][CH2:26][NH:25][CH2:24][CH2:23]1)[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1.[CH:28](OC(C)C)(C)C>>[OH:1][C:2]1[CH:3]=[CH:4][C:5]2[N:9]=[C:8]([C:10]([N:25]3[CH2:24][CH2:23][CH:22]([CH2:15][C:16]4[CH:17]=[CH:18][C:19]([CH3:28])=[CH:20][CH:21]=4)[CH2:27][CH2:26]3)=[O:12])[NH:7][C:6]=2[CH:13]=1参加物
4
実験手順
The title compound is prepared from 6-hydroxy-1H-benzoimidazole-2-carboxylic acid [Example elözö d] and 4-(-methylbenzyl)piperidine [J. Org. Chem., 64, 3763 (1999)] according to the method described in Example 25. Mp.: 93° C. (diisopropyl ether).
出典と根拠
- ORDレコード
- ord-73e45b30a2de4d5da93828b290ae6aea
- 出典データセット
- uspto-grants-2005_07