Ethyl indole-2-carboxylate → 3-(Dimethylaminophenylmethyl)-1H-indole-2-carboxylic Acid Ethyl Ester
反応式
[CH2:1]([O:3][C:4]([C:6]1[NH:7][C:8]2[C:13]([CH:14]=1)=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:5])[CH3:2].[Cl-].[CH:16](=[N+:23]([CH3:25])[CH3:24])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[CH2:1]([O:3][C:4]([C:6]1[NH:7][C:8]2[C:13]([C:14]=1[CH:16]([N:23]([CH3:25])[CH3:24])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:5])[CH3:2]参加物
3
実験手順
The preparation was carried out in accordance with general synthesis instructions 4 from 1H-indole-2-carboxylic acid ethyl ester and benzylidene-dimethyl-ammonium chloride. For characterization, an ESI-MS was recorded:
出典と根拠
- ORDレコード
- ord-72da6cfad289430d96716ceae4346d94
- 出典データセット
- uspto-grants-2006_08
- 特許番号
- US07091220B2
反応ノート
読み込み中…