2-Methylindole → Dimethyl-[(2-methyl-1H-indol-3-yl)-phenylmethyl]-amine

反応式

[CH3:1][C:2]1[NH:3][C:4]2[C:9]([CH:10]=1)=[CH:8][CH:7]=[CH:6][CH:5]=2.[Cl-].[CH:12](=[N+:19]([CH3:21])[CH3:20])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[CH3:20][N:19]([CH3:21])[CH:12]([C:10]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[NH:3][C:2]=1[CH3:1])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

参加物

反応物 2

HCID 72242-Methylindole

HCID 11073839Methanaminium, N-methyl-N-(phenylmethylene)-, chloride

生成物 1

HCID 9921470Dimethyl-[(2-methyl-1H-indol-3-yl)-phenylmethyl]-amine

実験手順

The preparation was carried out in accordance with general synthesis instructions 4 from 2-methyl-1H-indole and benzylidene-dimethyl-ammonium chloride, which had been prepared in accordance with example 1.

後処理

customhad been prepared in accordance with example 1

出典と根拠

ORDレコード: ord-e385ae51537746cd8962eb40b5c4ef0d
出典データセット: uspto-grants-2006_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07091220B2

反応ノート

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