化工社化工社 化学情報印刷レポート · 研究参考用
Water → Perindopril erbumine monohydrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Perindopril Erbumine | HCID 441313 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | Perindopril erbumine monohydrate | HCID 9847044 | — |
反応手順
Perindopril erbumine (5 gms) was suspended in acetonitrile (75 ml). To this was added water (0.4 ml) and the contents heated to dissolve the solids and cooled to 0 EC. The resulting slurry was filtered to obtain perindopril erbumine monohydrate (2.9 gms).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07351840B2 |
| 出典データセット | uspto-grants-2008_04 |
| ORD ID | ord-5a42d62a17dd43a8b107ff4b4ae0b469 |
| 出典メモ | uspto-grants-2008_04 |