化工社化工社 化学情報印刷レポート · 研究参考用
Perindopril Erbumine → Perindopril erbumine monohydrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Perindopril Erbumine | HCID 441313 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | Perindopril erbumine monohydrate | HCID 9847044 | 163.3% |
反応手順
Perindopril erbumine (20 gms) was suspended in ethyl acetate (300 ml). The contents were heated to dissolve the solids and cooled to 10 EC. The resulting slurry was filtered and dried in air having a relative humidity of at least 75% to give perindopril erbumine monohydrate (17 gms).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07351840B2 |
| 出典データセット | uspto-grants-2008_04 |
| ORD ID | ord-a699c9ecef724a7c98932c97321fce17 |
| 出典メモ | uspto-grants-2008_04 |