Propanenitrile, 3-(methylamino)- → N-(2-cyanoethyl)-N-methyl-2-(trifluoromethyl)benzenesulphonamide

HRID 901073

反応式

HRID 901073 の反応式
[F:1][C:2]([F:14])([F:13])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[S:9](Cl)(=[O:11])=[O:10].[CH3:15][NH:16][CH2:17][CH2:18][C:19]#[N:20]>>[C:19]([CH2:18][CH2:17][N:16]([CH3:15])[S:9]([C:4]1[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=1[C:2]([F:14])([F:13])[F:1])(=[O:11])=[O:10])#[N:20]

参加物

3

反応物 2

HCID 69656Propanenitrile, 3-(methylamino)-HCID 1366162-Trifluoromethylbenzenesulphonyl chloride

生成物 1

HCID 43084128N-(2-cyanoethyl)-N-methyl-2-(trifluoromethyl)benzenesulphonamide

実験手順

In operating analogously to Preparation V, starting with 2-(trifluoromethyl)benzenesulphonyl chloride and 3-(methylamino)propionitrile, the expected product is obtained as a yellow oil (yield=98%).

後処理

  1. customIn operating analogously to Preparation V

出典と根拠

ORDレコード
ord-1637b96defe1476fb9d1cdac926f88e7
出典データセット
uspto-grants-2008_04
特許番号
US07361687B2

関連ノート

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