Hydrochloric Acid → HCID 23134841、化合物
反応式
C([O:3][C:4](=[O:28])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][O:18][C:19]2[CH:24]=[C:23]([F:25])[C:22]([F:26])=[C:21]([F:27])[CH:20]=2)=[CH:7][CH:6]=1)C.[OH-].[Na+].Cl>O1CCOCC1>[F:25][C:23]1[CH:24]=[C:19]([CH:20]=[C:21]([F:27])[C:22]=1[F:26])[O:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][O:11][C:8]1[CH:9]=[CH:10][C:5]([C:4]([OH:28])=[O:3])=[CH:6][CH:7]=1参加物
5
実験手順
2.75 g of 4-[6-(3,4,5-Trifluoro-phenoxy)-hexyloxy]-benzoic acid ethyl ester was dissolved in 100 ml of 1,4-dioxane, and then 100 ml of a 1.0M NaOH solution was added thereto. After stirring for one day, the reaction solution was acidified with a 10% HCl solution and filtered to obtain a solid. The solid was recrystallized from ethanol to afford 4-[6-(3,4,5-trifluoro-phenoxy)-hexyloxy]-benzoic acid (yield: 62%).