Ethanol → HCID 23338142、化合物

HRID 903321ノート

反応式

HRID 903321 の反応式
[Na].ClC1N=NN=C(Cl)C=1.[Cl:10][C:11]1[N:16]=[C:15](Cl)[N:14]=[C:13]([N:18]([CH3:20])[CH3:19])[N:12]=1.[CH2:21]([OH:23])[CH3:22]>>[Cl:10][C:11]1[N:16]=[C:15]([O:23][CH2:21][CH3:22])[N:14]=[C:13]([N:18]([CH3:20])[CH3:19])[N:12]=1

参加物

5

反応物 4

HCID 702Ethanol2 回HCID 169852,4-Dichloro-6-(dimethylamino)-1,3,5-triazineHCID 5360545SodiumHCID 18348308HCID 18348308、化合物

生成物 1

HCID 23338142HCID 23338142、化合物

実験手順

A solution of sodium (0.46 g.) in ethanol (50 ml.) was added with stirring and waterbath cooling (25° C.) to a solution of the dichlorotriazine (3.86 g.) from (a) in ethanol (50 ml.). Following the addition the solution was poured into ice water (250 ml.) and the product collected, dried and crystallised from petroleum as needles (2.5 g.) having a melting point of 124° C.

後処理

  1. additionthe addition the solution
  2. customthe product collected
  3. customdried
  4. customcrystallised from petroleum as needles (2.5 g.)

出典と根拠

ORDレコード
ord-66b37f85eaa14fb1b300dbb4ab41495e
出典データセット
uspto-grants-1980_10
特許番号
US04226990

反応ノート

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