Trifluoroacetic acid → HCID 178508837、化合物

HRID 905504

反応式

HRID 905504 の反応式
[NH2:1][C:2]1[N:6]=[C:5]([NH2:7])[NH:4][N:3]=1.[F:8][C:9]([F:14])([F:13])[C:10]([OH:12])=[O:11]>O>[O-:12][C:10]([C:9]([F:14])([F:13])[F:8])=[O:11].[NH2:1][C:2]1[NH:3][NH+:4]=[C:5]([NH2:7])[N:6]=1

参加物

4

反応物 2

HCID 6422Trifluoroacetic acidHCID 150783,5-Diamino-1,2,4-triazole

生成物 1

HCID 178508837HCID 178508837、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

3,5-Diamino-1,2,4-triazole (1.50 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

後処理

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C. for 4 hours

出典と根拠

ORDレコード
ord-e08f5efc7a6e4caaaed595895ce16a64
出典データセット
uspto-grants-2011_09
特許番号
US08012277B2

関連ノート

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