benzyl (2S,3S)-3-hydroxy-2-methyl-3-propylpyrrolidine-1-carboxylate → (2S,3S)-2-methyl-3-propylpyrrolidin-3-ol
反応式
[OH:1][C@@:2]1([CH2:18][CH2:19][CH3:20])[CH2:6][CH2:5][N:4](C(OCC2C=CC=CC=2)=O)[C@H:3]1[CH3:17]>[Pd].O>[CH3:17][C@H:3]1[C@@:2]([CH2:18][CH2:19][CH3:20])([OH:1])[CH2:6][CH2:5][NH:4]1参加物
4
実験手順
By an operation in the same manner as in Reference Example 4 and using benzyl (2S,3S)-3-hydroxy-2-methyl-3-propylpyrrolidine-1-carboxylate (2.32 g) and 50% water containing-10% Pd/C (0.10 g), the title compound was obtained as a colorless solid (yield: 1.50 g, yield: 96%).
出典と根拠
- ORDレコード
- ord-aef86ca39d554a07b6f98f2933e81b32
- 出典データセット
- uspto-grants-2011_09
- 特許番号
- US08013008B2
反応ノート
読み込み中…