Ammonium Hydroxide → 2,2-Diethoxyacetamide

HRID 907378

反応式

HRID 907378 の反応式
[CH2:1]([O:3][CH:4]([O:10][CH2:11][CH3:12])[C:5](OCC)=[O:6])[CH3:2].[NH4+:13].[OH-]>>[CH2:1]([O:3][CH:4]([O:10][CH2:11][CH3:12])[C:5]([NH2:13])=[O:6])[CH3:2]

参加物

3

反応物 2

HCID 14923Ammonium HydroxideHCID 80169Ethyl diethoxyacetate

生成物 1

HCID 1007652,2-Diethoxyacetamide収率 99%

実験手順

Ethyl diethoxyacetate (Aldrich) (10 mL, 56.41 mmol) was added to concentrated NH4OH (50 mL) and the mixture allowed to stir until a homogeneous solution was obtained (40 hours). The solvent was then removed under reduced pressure to yield the sub-title compound as fine white needles (8.209 g, 99%).

後処理

  1. customwas obtained (40 hours)
  2. customThe solvent was then removed under reduced pressure

出典と根拠

ORDレコード
ord-3c948a6daead4d7a9f915b6f7b70559c
出典データセット
uspto-grants-2011_09
特許番号
US08012967B2

関連ノート

読み込み中…