関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrazine | HCID 9321 | — |
| 反応物 | Methyl cyclohexanecarboxylate | HCID 20748 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Cyclohexanecarbohydrazide | HCID 240039 | 33.5% |
反応手順
To a solution of methyl cyclohexane carboxylate (12 g, 83.9 mmol) in MeOH (50 mL) was added hydrazine (5.3 mL, 1.67 mol). The reaction mixture was heated at 65° C. overnight. The reaction mixture was cooled to room temperature and the resultant solid was collected by filtration and was dried in vacuo to give 4.0 g of cyclohexanecarboxylic acid hydrazide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07265104B2 |
|---|
| 出典データセット | uspto-grants-2007_09 |
|---|
| ORD ID | ord-6a7b9941cf344e88a3a9300997f059c2 |
|---|
| 出典メモ | uspto-grants-2007_09 |
|---|
