関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Dimethyloctadecylamine | HCID 15365 | — |
| 反応物 | (3-Chloropropyl)triethoxysilane | HCID 78771 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Triethoxysilylpropyl steardimonium chloride | HCID 9807252 | 150.4% |
反応手順
Firstly, 41.5 g (0.17 moL) of triethoxysilylpropyl chloride (Tokyo Kasei Kogyo Co., Ltd.), 44.6 g (0.150 moL) of N,N-dimethyl octadecylamine (Tokyo Kasei Kogyo Co., Ltd.) and 40.5 g of ethanol are fed into a nitrogen-purged pressurized reactor and heated to 135° C. After the reaction for 20 hours, 121.4 g of dimethyloctadecyl[3-(triethoxysilyl)propyl]ammonium chloride (EtAC) in ethanol solution is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US09278107B2 |
|---|
| 出典データセット | uspto-grants-2016_03 |
|---|
| ORD ID | ord-5bceff8534ce4e3e8af18bec98044369 |
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| 出典メモ | uspto-grants-2016_03 |
|---|
