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HRID921976

反应详情

EQUATION

反应方程式

HRID 921976 的结构方程式

REACTANTS

反应物

2
结构：CCCCCCCCCCCCCCCCCCN(C)C
HCID15365

N,N-Dimethyl-1-octadecanamine

C20H43N

结构：CCO[Si](CCCCl)(OCC)OCC
HCID78771

(3-Chloropropyl)(triethoxy)silane

C9H21ClO3Si

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCCCCCCC[N+](C)(C)CCC[Si](OCC)(OCC)OCC.[Cl-]
HCID9807252

N,N-Dimethyl-N-[3-(triethoxysilyl)propyl]octadecan-1-aminium chloride

C29H64ClNO3Si

收率 150.4%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

2 次

CONDITIONS

反应条件

温度
135 °C

PROCEDURE

实验过程

Firstly, 41.5 g (0.17 moL) of triethoxysilylpropyl chloride (Tokyo Kasei Kogyo Co., Ltd.), 44.6 g (0.150 moL) of N,N-dimethyl octadecylamine (Tokyo Kasei Kogyo Co., Ltd.) and 40.5 g of ethanol are fed into a nitrogen-purged pressurized reactor and heated to 135° C. After the reaction for 20 hours, 121.4 g of dimethyloctadecyl[3-(triethoxysilyl)propyl]ammonium chloride (EtAC) in ethanol solution is obtained.

WORKUP

后处理

  1. custompurged
  2. customAfter the reaction for 20 hours