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2,2-Dimethyl-1,3-dioxane-4,6-dione → 5-(4-(1H-1,2,4-triazol-1-yl)benzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

HRID 926565
ノート
印刷プレビュー

反応式

HRID 926565 の反応式
N1CCC[C@H]1C(O)=O.[N:9]1([C:14]2[CH:21]=[CH:20][C:17]([CH:18]=O)=[CH:16][CH:15]=2)[CH:13]=[N:12][CH:11]=[N:10]1.N1(C2C=CC(CC(C(O)=O)C(O)=O)=CC=2)C=NC=N1.[CH3:41][C:42]1([CH3:50])[O:47][C:46](=[O:48])[CH2:45][C:44](=[O:49])[O:43]1.CC1NC(C)=C(C(OCC)=O)CC=1C(OCC)=O>C(O)C.C(O)(C)C>[N:9]1([C:14]2[CH:21]=[CH:20][C:17]([CH2:18][CH:45]3[C:46](=[O:48])[O:47][C:42]([CH3:50])([CH3:41])[O:43][C:44]3=[O:49])=[CH:16][CH:15]=2)[CH:13]=[N:12][CH:11]=[N:10]1
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

8

反応物 5

HCID 162492,2-Dimethyl-1,3-dioxane-4,6-dioneHCID 70849Hantzsch esterHCID 145742L-ProlineHCID 27764884-(1H-1,2,4-triazol-1-yl)benzaldehydeHCID 867156252-(4-(1H-1,2,4-triazol-1-yl)benzyl)malonic acid

生成物 1

HCID 867156245-(4-(1H-1,2,4-triazol-1-yl)benzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

試薬・触媒・溶媒 2

HCID 702Ethanol溶媒HCID 3776Isopropanol溶媒

反応条件

温度
23 °C

実験手順

L-Proline (1.81 g, 15.6 mmol) was added to a stirring, heterogeneous mixture of 4-(1H-1,2,4-triazol-1-yl)benzaldehyde (13.5 g, 78.0 mmol, Intermediate 82: step a) and 2,2-dimethyl-1,3-dioxane-4,6-dione (11.2 g, 78.0 mmol) in ethanol (520 mL) at 23° C. After 1.5 hours, diethyl 1,4-dihydro-2,6-dimethyl-3,5-pyridinedicarboxylate (19.7 g, 78.0 mmol) was added in one portion. After 16 hours, the ethanol was removed by rotary evaporation at 35° C. to afford a yellow solid. Isopropanol (300 mL) was added and the heterogeneous mixture was stirred for 10 minutes at 23° C. The mixture was filtered and the filter cake was washed with isopropanol (150 mL). The solids were collected and dried under vacuum to provide the titled compound as a white solid.

後処理

  1. customat 23° C
  2. waitAfter 16 hours
  3. customthe ethanol was removed by rotary evaporation at 35° C.
  4. customto afford a yellow solid
  5. filtrationThe mixture was filtered
  6. washthe filter cake was washed with isopropanol (150 mL)
  7. customThe solids were collected
  8. customdried under vacuum

出典と根拠

ORDレコード
ord-c41f05ce4cf746899a384443f25e3e3a
出典データセット
uspto-grants-2016_03
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US09284308B2

反応ノート

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