Thionyl Chloride → 2-(4-ethoxyphenyl)acetyl Chloride

HRID 929736

反応式

HRID 929736 の反応式
[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][C:7]([CH2:10][C:11]([OH:13])=O)=[CH:6][CH:5]=1)[CH3:2].S(Cl)([Cl:16])=O>>[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][C:7]([CH2:10][C:11]([Cl:16])=[O:13])=[CH:6][CH:5]=1)[CH3:2]

参加物

3

反応物 2

HCID 24386Thionyl ChlorideHCID 78631Benzeneacetic acid, 4-ethoxy-

生成物 1

HCID 116297822-(4-ethoxyphenyl)acetyl Chloride

反応条件

温度
70 °C

実験手順

4-Ethoxyphenylacetic acid (0.5 g, 2.8 mmol) was transferred to a 7 ml vial and dissolved in thionylchloride (3 ml). The reaction mixture was shaken at 70° C. for 21/2 hours. Thionylchloride was evaporated off and the resulting product was used unpurified.

後処理

  1. customThionylchloride was evaporated off

出典と根拠

ORDレコード
ord-06de92c37c804f80ad9dfd09f1479dee
出典データセット
uspto-grants-2016_03
特許番号
US09296694B2

関連ノート

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