1,2-Dichlorohexafluorocyclobutane → 1-Chloro 3,3,4,4-tetrafluoro cyclobutene

HRID 963798

反応式

HRID 963798 の反応式
[Cl:1][C:2]1(F)[C:5]([F:7])([F:6])[C:4]([F:9])([F:8])[C:3]1(F)Cl.FC1(F)C(F)=C(F)C1(F)F>>[F:6][C:5]1([F:7])[C:2]([Cl:1])=[CH:3][C:4]1([F:9])[F:8]

参加物

3

実験手順

The conversion of 1,2-dichlorohexafluorocyclobutane was 30%, the selectivity of the targeted hexafluorocyclobutene was 96% and a 3.5% selectivity of tetrafluoro-1-chlorocyclobutene was formed as the by-product. The selectivity and the conversion were calculated by multiplying the correction coefficient, which was independently determined by the gas chromatography peak areas. The same procedure was used for the following operations.

出典と根拠

ORDレコード
ord-aba3804530b64007a937b59926300bb1
出典データセット
uspto-grants-1998_06
特許番号
US05763703

関連ノート

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