Dibutyl Phthalate → 2-Hydroxyethyl Methacrylate

HRID 965267ノート

反応式

HRID 965267 の反応式
CCCCCCCC(OOC(C)(C)C)=[O:9].C(OCCCC)(=O)[C:17]1[C:18](=[CH:26]C=CC=1)[C:19]([O:21][CH2:22][CH2:23]CC)=[O:20]>>[C:19]([O:21][CH2:22][CH2:23][OH:9])(=[O:20])[C:18]([CH3:17])=[CH2:26]

参加物

3

反応物 2

HCID 3026Dibutyl PhthalateHCID 83499tert-Butyl peroctoate

生成物 1

HCID 133602-Hydroxyethyl Methacrylate

実験手順

2 h after the end of the addition, 1 g of tert-butyl peroctoate is fed in. The total polymerization time is 8 h. After the end of polymerization, the mixture is diluted with 590.0 g of dibutyl phthalate. An almost clear, viscous solution is obtained.

後処理

  1. customAfter the end of polymerization
  2. customAn almost clear, viscous solution is obtained

出典と根拠

ORDレコード
ord-4e8d258d76fe4ab7af350548402b97c8
出典データセット
uspto-grants-1998_06
特許番号
US05773505

反応ノート

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