Thymine → HCID 54034076、化合物

HRID 965321ノート

反応式

HRID 965321 の反応式
[CH2:1]([O:3][C:4](=[O:20])[CH:5]([N:17]=[C:18]=[O:19])[CH2:6][CH2:7][CH2:8][NH:9][C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])[CH3:2].[NH:21]1[CH:29]=[C:27]([CH3:28])[C:25](=[O:26])[NH:24][C:22]1=[O:23]>>[CH2:1]([O:3][C:4](=[O:20])[CH:5]([NH:17][C:18]([N:21]1[CH:29]=[C:27]([CH3:28])[C:25](=[O:26])[NH:24][C:22]1=[O:23])=[O:19])[CH2:6][CH2:7][CH2:8][NH:9][C:10]([O:12][C:13]([CH3:14])([CH3:15])[CH3:16])=[O:11])[CH3:2]

参加物

3

反応物 2

HCID 1135ThymineHCID 54358079HCID 54358079、化合物

生成物 1

HCID 54034076HCID 54034076、化合物

実験手順

The reaction solution from Example 10 is placed in a flask and to this is added thymine (12.6 g, 0.1 mol) . The resulting solution is allowed to stir for 12 hours, then is evaporated to a solid, which is purified by column chromatography using dichlormethane:ethanol as the eluent.

後処理

  1. customis evaporated to a solid, which
  2. customis purified by column chromatography

出典と根拠

ORDレコード
ord-97bb628d686c43858b1c82085d00f209
出典データセット
uspto-grants-1998_06
特許番号
US05773571

反応ノート

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