化工社化工社 化学情報印刷レポート · 研究参考用
2-Mesityl-3-nitropyridine → 2-Mesityl-3-pyridinamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Mesityl-3-nitropyridine | HCID 22249491 | — |
| 触媒 | HCID 178418390 | HCID 178418390 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 溶媒 | HCID 178418361 | HCID 178418361 | — |
| 生成物 | 2-Mesityl-3-pyridinamine | HCID 16741426 | 106.5% |
反応手順
Palladium-carbon (10%, 0.6 g) was added to a solution of 2-mesityl-3-nitropyridine (5.99 g, 23 mmol) in ethanol (120 mL), followed by stirring for one day in hydrogen atmospher. The mixture was filtered through Celite and evaporated, to give the title compound (5.2 g) as white crystals.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06951865B2 |
| 出典データセット | uspto-grants-2005_10 |
| ORD ID | ord-c73ee1167547434ca4212285a5e42e77 |
| 出典メモ | uspto-grants-2005_10 |