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Ethyl (4-mercapto-2-methylphenoxy)acetate → Ethyl{2-methyl-4-[({3-methyl-5-[4-(trifluoromethoxy)phenyl]thien-2-yl}methyl)thio]phenoxy}acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl (4-mercapto-2-methylphenoxy)acetate | HCID 16641178 | — |
| 反応物 | {3-Methyl-5-[4-(trifluoromethoxy)phenyl]thien-2-yl}methanol | HCID 21986356 | — |
| 反応物 | Ethyl{2-methyl-4-[({5-[4-(trifluoromethyl)phenyl]-3-furyl}methyl)thio]phenoxy}acetate | HCID 21986477 | — |
| 生成物 | Ethyl{2-methyl-4-[({3-methyl-5-[4-(trifluoromethoxy)phenyl]thien-2-yl}methyl)thio]phenoxy}acetate | HCID 21986465 | — |
反応手順
The title compound was prepared by a method analogous to that used for the preparation of ethyl{2-methyl-4-[({5-[4-(trifluoromethyl)phenyl]-3-furyl}methyl)thio]phenoxy}acetate (example 1) using ethyl(4-mercapto-2-methylphenoxy)acetate (intermediate 4) and {3-methyl-5-[4-(trifluoromethoxy)phenyl]thien-2-yl}methanol (intermediate 118).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07091237B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-2e54c38b1900406b95a26d375bd2588c |
| 出典メモ | uspto-grants-2006_08 |