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Triethylamine → HCID 178422384、化合物

HRID 970155
ノート
印刷プレビュー

反応式

HRID 970155 の反応式
BrC1C(C)=[C:4]([C:12]2[CH2:16][CH2:15]ON=2)[C:5]([S:8](C)(=[O:10])=[O:9])=[CH:6][CH:7]=1.[CH3:18][N:19]1[C:23]([OH:24])=[CH:22][CH:21]=[N:20]1.[C:25](=[O:28])([O-])[O-].[K+].[K+].C([N:33]([CH2:36][CH3:37])CC)C.C1(P(C2C=CC=CC=2)C2C=CC=CC=2)C=CC=CC=1.[O:57]1[CH2:62][CH2:61]OCC1>[Pd](Cl)Cl>[CH3:18][N:19]1[C:23]([OH:24])=[C:22]([C:25](=[O:28])[C:12]2[C:16]([CH3:15])=[C:37]([C:36]3[CH2:61][CH2:62][O:57][N:33]=3)[CH:6]([CH3:7])[C:5](=[S:8](=[O:10])=[O:9])[CH:4]=2)[CH:21]=[N:20]1
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

8

反応物 6

HCID 8471TriethylamineHCID 11430Potassium CarbonateHCID 11776TriphenylphosphineHCID 312751,4-DioxaneHCID 109470753-(3-Bromo-2-methyl-6-(methylsulfonyl)phenyl)-4,5-dihydroisoxazoleHCID 178481816HCID 178481816、化合物

生成物 1

HCID 178422384
HCID 178422384、化合物

試薬・触媒・溶媒 1

HCID 24290Palladium Chloride触媒

反応条件

温度
130 °C

実験手順

2 l of 1,4-dioxane, 250 g (0.77 mol) of 3-(3-bromo-2-methyl-6-methylsulfonylphenyl)-4,5-dihydroisoxazole, 77 g (0.77 mol) of 1-methyl-5-hydroxypyrazole, 269 g (1.93 mol) of potassium carbonate, 197 g (1.93 mol) of triethylamine, 1.39 g (0.0077 mol) of palladium(II) chloride and 4.12 g (0.0154 mol) of triphenylphosphine were added to a 3.5 l autoclave. The autoclave was washed twice with nitrogen, the mixture was heated with stirring to 130° C. and a carbon monoxide pressure of 6 kg/cm2 was applied. By continuous addition of carbon monoxide, the carbon monoxide pressure was kept constant at 6 kg/cm2 and the mixture was stirred at 130° C. for 36 h. The mixture was then admixed with 1 l of demineralized water and the precipitated palladium was filtered off over a blue-band filter (pore size 2 to 3 μ) and washed with water. Dioxane, triethylamine and some of the water were then distilled off in one step (150 mbar or atmospheric pressure). The aqueous phase was adjusted to pH 2.5 using 20% strength sulfuric acid and stirred at 5° C. for 12 h, while the pH was being readjusted. The precipitate was filtered off, washed three times with water and dried at 70° C. under reduced pressure. This gave 227 g of product (calc. 100%).

後処理

  1. washThe autoclave was washed twice with nitrogen
  2. temperaturethe mixture was heated
  3. additionBy continuous addition of carbon monoxide
  4. stirringthe mixture was stirred at 130° C. for 36 h
  5. filtrationthe precipitated palladium was filtered off over a blue-band filter (pore size 2 to 3 μ)
  6. washwashed with water
  7. distillationDioxane, triethylamine and some of the water were then distilled off in one step (150 mbar or atmospheric pressure)
  8. stirringstirred at 5° C. for 12 h, while the pH
  9. filtrationThe precipitate was filtered off
  10. washwashed three times with water
  11. customdried at 70° C. under reduced pressure

出典と根拠

ORDレコード
ord-993aceb1fde547ee89b1730f8716e5b9
出典データセット
uspto-grants-2007_12
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US07309802B2

反応ノート

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