反応式
[C:1]([Cl:4])(Cl)=[CH2:2].[C:5]([O:9]C)(=[O:8])[CH:6]=[CH2:7].[CH2:11]([C:13](C)=[O:14])[CH3:12]>>[C:5]([OH:9])(=[O:8])[CH:6]=[CH2:7].[Cl:4][CH2:1][C:2]([O:14][CH2:13][CH:11]=[CH2:12])=[O:8]参加物
5
実験手順
Vinylidene chloride (60.5g) was mixed together with 28.8. of methyl acrylate. 10.6 g of acrylic acid and 11.1 g of allyl monochloroacetate in 100 ml of methyl ethyl ketone to give a 50% by volume solution, the temperature of the methyl ethyl ketone being 40° C. Then as copolymerisation initiator 1.0 g of 2, 2'- azobisisobutyronitrile was added to the monomer solution. The solution was maintained at 40° C until the copolymerisation was complete, which took 6 days.
出典と根拠
- ORDレコード
- ord-0b7d9ba02a0348b8864b5058b14de80c
- 出典データセット
- uspto-grants-1977_10
- 特許番号
- US04052528
関連ノート
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