Hydrochloric Acid → 2-Amino-6-dimethylaminobenzonitrile
反応式
[CH3:1][N:2]([CH3:14])[C:3]1[CH:10]=[CH:9][CH:8]=[C:7]([N+:11]([O-])=O)[C:4]=1[C:5]#[N:6].Cl>[Fe].CO>[NH2:11][C:7]1[CH:8]=[CH:9][CH:10]=[C:3]([N:2]([CH3:14])[CH3:1])[C:4]=1[C:5]#[N:6]参加物
5
実験手順
To a suspension of 5.7 g. of 2-dimethylamino-6-nitrobenzonitrile in 20 ml. of methanol and 17 ml. of concentrated hydrochloric acid is added 5.3 g. of iron powder in portions. The mixture is stirred for 1/2 hour, diluted with 200 ml. of water and extracted with methylene chloride which is dried and evaporated in vacuo to yield crude 2-amino-6-dimethylaminobenzonitrile.
後処理
- additionTo a suspension of 5.7 g
- additiondiluted with 200 ml
- extractionof water and extracted with methylene chloride which
- customis dried
- customevaporated in vacuo
出典と根拠
- ORDレコード
- ord-7e201ebe092c4213b63b65dd74a340dd
- 出典データセット
- uspto-grants-1977_10
- 特許番号
- US04054591
反応ノート
読み込み中…