Thionyl Chloride → [3-(Trifluoromethyl)phenoxy]acetyl chloride
反応式
[F:1][C:2]([F:15])([F:14])[C:3]1[CH:4]=[C:5]([CH:11]=[CH:12][CH:13]=1)[O:6][CH2:7][C:8](O)=[O:9].S(Cl)([Cl:18])=O>>[F:1][C:2]([F:15])([F:14])[C:3]1[CH:4]=[C:5]([CH:11]=[CH:12][CH:13]=1)[O:6][CH2:7][C:8]([Cl:18])=[O:9]参加物
3
実験手順
A solution of 6 g of the product of Step B in 36 ml of thionyl chloride was refluxed with stirring for one hour and was evaporated to dryness under reduced pressure to obtain 6.44 g of the desired product which was used as is for the next step.
後処理
- customwas evaporated to dryness under reduced pressure
出典と根拠
- ORDレコード
- ord-c09db5187a1f4a44a6e4420e23b35327
- 出典データセット
- uspto-grants-1991_11
- 特許番号
- US05064861
反応ノート
読み込み中…