Ammonia → 2-Amino-4-chlorobenzamide

HRID 973914

反応式

HRID 973914 の反応式
Cl[C:2]1[CH:10]=[C:9]([Cl:11])[CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5].[NH3:12]>>[NH2:12][C:2]1[CH:10]=[C:9]([Cl:11])[CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5]

参加物

3

反応物 2

HCID 222AmmoniaHCID 755562,4-Dichlorobenzamide

生成物 1

HCID 123748372-Amino-4-chlorobenzamide

実験手順

190 g of 2,4-dichlorobenzamide was dissolved in 1.5 liters of aqueous ammonia, and to the resulting solution was added 100 g of cuprous chloride. The mixture was reacted at 80° C. for 15 hours in an autoclave, and then neutralized. The crystals deposited were collected by filtration. Yield: 122 g (71.5%)

後処理

  1. customThe mixture was reacted at 80° C. for 15 hours in an autoclave
  2. filtrationThe crystals deposited were collected by filtration

出典と根拠

ORDレコード
ord-70f469c15fe2496a9d058d1f1845b271
出典データセット
uspto-grants-1991_11
特許番号
US05066577

関連ノート

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