化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → 2-Amino-4-chlorobenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | 2,4-Dichlorobenzamide | HCID 75556 | — |
| 生成物 | 2-Amino-4-chlorobenzamide | HCID 12374837 | — |
反応手順
190 g of 2,4-dichlorobenzamide was dissolved in 1.5 liters of aqueous ammonia, and to the resulting solution was added 100 g of cuprous chloride. The mixture was reacted at 80° C. for 15 hours in an autoclave, and then neutralized. The crystals deposited were collected by filtration. Yield: 122 g (71.5%)
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05066577 |
| 出典データセット | uspto-grants-1991_11 |
| ORD ID | ord-70f469c15fe2496a9d058d1f1845b271 |
| 出典メモ | uspto-grants-1991_11 |