4-Fluorobenzylamine → HCID 20222900、化合物
反応式
[N:1]([CH2:4][CH:5]([O:8][CH3:9])[O:6][CH3:7])=[C:2]=[S:3].[F:10][C:11]1[CH:16]=[CH:15][C:14]([CH2:17][NH2:18])=[CH:13][CH:12]=1>O1CCCC1>[CH3:7][O:6][CH:5]([O:8][CH3:9])[CH2:4][NH:1][C:2]([NH:18][CH2:17][C:14]1[CH:15]=[CH:16][C:11]([F:10])=[CH:12][CH:13]=1)=[S:3]参加物
4
実験手順
A mixture of 4.8 parts of 1-isothiocyanato-2,2-dimethoxyethane, 4.2 parts of 4-fluorobenzenemethanamine and 90 parts of tetrahydrofuran was stirred overnight. The reaction mixture was evaporated, yielding 8.9 parts (99%) of N-(2,2-dimethoxyethyl)-N'-[(4-fluorophenyl)methyl]thiourea (188).
後処理
- customThe reaction mixture was evaporated
出典と根拠
- ORDレコード
- ord-9bd70976f211457cba8a73591c25974b
- 出典データセット
- uspto-grants-1987_01
- 特許番号
- US04634704
反応ノート
読み込み中…