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2-Methyl-1-pentanol → Magnesium 2-methyl-1-pentyloxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methyl-1-pentanol | HCID 7745 | — |
| 反応物 | Heptane | HCID 8900 | — |
| 反応物 | Butyllithium | HCID 178418339 | — |
| 反応物 | HCID 178448199 | HCID 178448199 | — |
| 溶媒 | Cyclohexane | HCID 8078 | — |
| 生成物 | Magnesium 2-methyl-1-pentyloxide | HCID 86741193 | — |
反応手順
To 10 ml of a solution of 4.33 ml of 2-methyl-1-pentanol in heptane there is added 0.4 ml of 1.91 Molar n-butyllithium in cyclohexane. To the cloudy mixture, there is added, slowly and with good mixing, 15 ml of a 1.036 Molar solution of n-butyl-sec-butylmagnesium in heptane. A clear, colorless, viscous solution of magnesium 2-methyl-1-pentyloxide is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04634786 |
| 出典データセット | uspto-grants-1987_01 |
| ORD ID | ord-13920a553d2d4184aef9eb05f8cdcda1 |
| 出典メモ | uspto-grants-1987_01 |