HRID980026

反应详情

EQUATION

反应方程式

HRID 980026 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To 10 ml of a solution of 4.33 ml of 2-methyl-1-pentanol in heptane there is added 0.4 ml of 1.91 Molar n-butyllithium in cyclohexane. To the cloudy mixture, there is added, slowly and with good mixing, 15 ml of a 1.036 Molar solution of n-butyl-sec-butylmagnesium in heptane. A clear, colorless, viscous solution of magnesium 2-methyl-1-pentyloxide is obtained.

WORKUP

后处理

  1. additionTo the cloudy mixture, there is added