Hydroxyacetonitrile → (Dodecylamino)acetonitrile

HRID 980862

反応式

HRID 980862 の反応式
O[CH2:2][C:3]#[N:4].[CH2:5]([NH2:17])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]>CO>[CH2:5]([NH:17][CH2:2][C:3]#[N:4])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

参加物

4

反応物 2

HCID 7857HydroxyacetonitrileHCID 13583Dodecylamine

生成物 1

HCID 222308(Dodecylamino)acetonitrile

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

In a flask of 500 ml provided with a magnetic stirrer, 4.56 gr of hydroxyacetonitrile (0.08 mol) were mixed at room temperature with 16.3 gr of dodecylamine (0.088 mol) in 250 ml of methanol. The mixture was allowed to stand for 16 hours at room temperature and methanol was evaporated. The obtained liquid was distilled under 10-2 mm Hg. The fraction distilling between 106° and 116° crystallizes after cooling.

後処理

  1. customIn a flask of 500 ml provided with a magnetic stirrer
  2. custommethanol was evaporated
  3. distillationThe obtained liquid was distilled under 10-2 mm Hg
  4. distillationThe fraction distilling between 106° and 116°
  5. customcrystallizes
  6. temperatureafter cooling

出典と根拠

ORDレコード
ord-062b5b872d41428695569fdb5abf608a
出典データセット
uspto-grants-1987_01
特許番号
US04639468

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