Sodium Hydroxide → 3,5-dimercaptobenzyl alcohol
反応式
CN(C)C([S:5][C:6]1[CH:7]=[C:8]([CH:11]=[C:12]([S:14]C(=O)N(C)C)[CH:13]=1)[CH2:9][OH:10])=O.[OH-].[Na+]>>[SH:5][C:6]1[CH:7]=[C:8]([CH:11]=[C:12]([SH:14])[CH:13]=1)[CH2:9][OH:10]参加物
3
実験手順
3,5-Bis (dimethylcarbamoylthio) benzyl alcohol was treated with sodium hydroxide according to the ordinary method to give 3,5-dimercaptobenzyl alcohol. This alcohol was then brominated in a manner similar to that in EXAMPLE 17, giving 3,5-dimercaptobenzyl bromide, followed by the reaction with urea according to the ordinary method giving 3,5-dimercaptobenzyl mercaptan.
出典と根拠
- ORDレコード
- ord-65f13128aa8d4aa78727b28b4c936985
- 出典データセット
- uspto-grants-2003_10
- 特許番号
- US06630578B2
反応ノート
読み込み中…