化工社化工社 化学情報印刷レポート · 研究参考用
Water → Acetic Acid 12-(4-Formyl-phenoxy)-dodecyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | 4-(12-Hydroxy-dodecyloxy)-benzaldehyde | HCID 22987548 | — |
| 生成物 | Acetic Acid 12-(4-Formyl-phenoxy)-dodecyl Ester | HCID 11244987 | — |
反応手順
4-(12-Hydroxyl-dodecyloxy)-benzaldehyde (1.1 g, 3.6 mmol, see Example 2 above) was heated at reflux in acetic anhydride (15 ml) for 90 minutes. After cooling, the solution was poured into water with stirring. The title compound formed as a precipitate which was collected by filtration, washed with water and dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06630128B1 |
| 出典データセット | uspto-grants-2003_10 |
| ORD ID | ord-f8fc0837b3a749fabb70322c2da38585 |
| 出典メモ | uspto-grants-2003_10 |