Mls000756500 → 3-Amino-N-3-pyridinylbenzamide
反応式
[N+:1]([C:4]1[CH:5]=[C:6]([CH:16]=[CH:17][CH:18]=1)[C:7]([NH:9][C:10]1[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=1)=[O:8])([O-])=O>C(O)C.[Pd]>[NH2:1][C:4]1[CH:5]=[C:6]([CH:16]=[CH:17][CH:18]=1)[C:7]([NH:9][C:10]1[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=1)=[O:8]参加物
4
実験手順
A solution of 3-(3-nitrobenzoylamino)-pyridine (2 g, 8.23 mmol) in ethanol (200 ml) was treated with 10% palladium on charcoal (0.5 g) and hydrogenated at atmospheric pressure for 4 h. Filtration and evaporation afforded the product as a white solid (1.51 g, 86%)
後処理
- filtrationFiltration and evaporation
出典と根拠
- ORDレコード
- ord-5612c0241b86421b83bede928603f868
- 出典データセット
- uspto-grants-2003_10
- 特許番号
- US06638953B2
反応ノート
読み込み中…