ホームMCPワークベンチSkills
ホームワークベンチ通知マイページ
llms.txt · MCPガイドプライバシーポリシー · 利用規約 · サポートv1.8.0
  1. ホーム
  2. /反応

Dichloromethane → N-piperidinopropyl-5-(3,4-dichlorophenyl)-3-methyl-pentadiene carboxamide

HRID 989782
ノート
印刷プレビュー

反応式

HRID 989782 の反応式
[Cl:1][C:2]1[CH:3]=[C:4]([CH:9]=[CH:10][C:11]([CH3:16])=[CH:12][C:13](O)=O)[CH:5]=[CH:6][C:7]=1[Cl:8].[CH2:17]([N:19]([CH2:22][CH3:23])[CH2:20][CH3:21])[CH3:18].ClC([O:27][CH2:28]C(C)C)=O.[N:32]1(NCCC)CCCC[CH2:33]1.[CH2:42](Cl)Cl>>[N:19]1([CH2:22][CH2:23][CH2:33][NH:32][C:28]([CH:13]=[CH:12][C:11]([CH3:16])=[CH:10][CH2:9][C:4]2[CH:5]=[CH:6][C:7]([Cl:8])=[C:2]([Cl:1])[CH:3]=2)=[O:27])[CH2:20][CH2:21][CH2:42][CH2:18][CH2:17]1
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

6

反応物 5

HCID 6344DichloromethaneHCID 8471TriethylamineHCID 62365Isobutyl chloroformateHCID 18419402Piperidino-propylamineHCID 858118935-(3,4-dichlorophenyl)-3-methyl-pentadienoic Acid

生成物 1

HCID 88175739N-piperidinopropyl-5-(3,4-dichlorophenyl)-3-methyl-pentadiene carboxamide

反応条件

温度
0 °C

実験手順

A suspension of 5-(3,4-dichlorophenyl)-3-methyl-pentadienoic acid (0.100 g, 0.390 mmol) in CH2Cl2 (5 mL) is treated with triethyl-amine (0.050 cr, 0.050 mmol) and cooled to 0° C. The resulting colorless solution is then treated with isobutyl chloroformate (0.065 g, 0.050 mmol). After 30 min., piperidino-propylamine (0.071 g, 0.050 mmol) is added, and the reaction mixture is allowed to warm to room temperature. After stirring overnight, the reaction mixture is quenched with aqueous sodium bicarbonate. The aqueous layer is extracted several times with CH2Cl2, and the combined organic layers are dried (sodium sulfate), and concentrated in vacuo. The residue is treated with excess methanolic HCl, evaporated in vacuo, and rinsed with ether to yield 0.159 g of a hygroscopic white solid, mp 50-60° C.

後処理

  1. temperatureto warm to room temperature
  2. customthe reaction mixture is quenched with aqueous sodium bicarbonate
  3. extractionThe aqueous layer is extracted several times with CH2Cl2
  4. dry with materialthe combined organic layers are dried (sodium sulfate)
  5. concentrationconcentrated in vacuo
  6. additionThe residue is treated with excess methanolic HCl
  7. customevaporated in vacuo
  8. washrinsed with ether

出典と根拠

ORDレコード
ord-b67944bef1b641c29bb85de48b76ef73
出典データセット
uspto-grants-2002_10
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US06458806B1

反応ノート

読み込み中…

このページの内容参加物反応条件実験手順後処理出典と根拠反応ノート